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利用气相色谱法测定腈纶中丙烯腈残留量

The residual amount of acrylonitrile in acrylic fiber was determined by gas chromatography

Modern Analytical Chemistry Research / 2019,1(1): 28-33 / 2019-12-27 759 775

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• Authors: 申子博     
• Information:

  延安大学，延安

• Keywords: Acrylonitrile; Gas chromatography; Mass spectrometry; Headspace solid phase microextraction 丙烯腈；气相色谱法；质谱法；顶空固相微萃取
• Abstract: In accordance with the European commission's ecological standards for the control of acrylonitrile residues in acrylic fibers, a headspace solid-phase extraction and chromatography-mass spectrometry (hs-smpe-gc /MS) technique was used to establish a method for the determination of acrylonitrile residues in acrylic fibers. The detection limit of this method is less than 0.5 mg/kg, and the recovery is between 91.9 % and 97.7 %. 依照欧盟委员会关于生态标准对腈纶中丙烯腈残留量的控制，采用顶 空固相萃取和色质谱联用技术（HS-SMPE-GC/MS），建立了腈纶中丙烯腈残 留量的测定方法。该方法检测限低于 0.5 mg/kg，回收率在 91.9 % ～ 97.7 % 之间。
• DOI: https://doi.org/10.35534/macr.0101005c
• Cite: 申子博．利用气相色谱法测定腈纶中丙烯腈残留量［J］．现代分析化学研究，2019，1（1）：28-33．