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Modern Analytical Chemistry Research
ISSN Print:2707-4765
ISSN Online:2707-4773
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2- 苯甲酰基 -3- 氯苯甲酸的合成表征
Synthesis and characterization of 2-benzoyl-3- chlorobenzoic acid
- Authors: 葛玲
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Information:
内蒙古化工职业学院，呼和浩特
- Keywords: 2-benzoyl-3-chlorobenzoic acid; 3-chlorophthalic anhydride; differential scanning calorimetry; infrared spectroscopy; mass spectrometry; 1H NMR 2- 苯甲酰基 -3- 氯苯甲酸；3- 氯代苯酐；差示扫描量热法；红外光 谱分析；质谱；核磁共振氢谱
- Abstract: In this paper, 2-benzoyl-3-chlorobenzoic acid was synthesized from 3-chlorophthalic anhydride and refined in ethyl acetate. The content of 2-benzoyl- 3-chlorobenzoic acid was 99.24%. Differential scanning calorimetry (DSC), infrared spectroscopy (IR), mass spectrometry (MS) and nuclear magnetic resonance (HNMR) were used to characterize 2-benzoyl-3-chlorobenzoic acid. 本文以 3- 氯代苯酐为原料合成 2- 苯甲酰基 -3- 氯苯甲酸粗品，然后 在乙酸乙酯中精制，得到的 2- 苯甲酰基 -3- 氯苯甲酸产品含量为 99.24%。采 用差示扫描量热法（DSC）、红外光谱 （IR）、质谱（MS）和核磁共振氢谱（HNMR） 等技术，对 2- 苯甲酰基 -3- 氯苯甲酸进行了表征。
- DOI: https://doi.org/10.35534/macr.0201001c
- Cite: 葛玲．2- 苯甲酰基 -3- 氯苯甲酸的合成表征［J］．现代分析化学研究，2020，2（1）：1-8．
